100 Years Setting the Tone
What
was once considered a worthless byproduct is now used to color paving
stones, concrete, and buildings all over the world. For 100 years, iron
oxide pigments have been produced at the LAUX plant in
Krefeld-Uerdingen—using a process that is unique worldwide. This is a
story about chemistry, the circular economy, and a highly interconnected
production network where scrap iron, experience, and teamwork come
together to create world-class pigments.
During
our visit, plant manager Holger Friedrich drinks his coffee from a mug
featuring the periodic table of elements. This is a small detail that
says a lot. Because when the manager of the reduction plant talks about
the LAUX process, it certainly doesn’t sound like business as usual.
“It’s almost like alchemy,” he says. Solid iron is machined; liquids
flow; gases are produced; heat is released. Substances change their
form—and a muddy, dark mass transforms into vibrant pigments of red,
black, or yellow. “Such a wide variety of processes—especially the
combination of inorganic and organic chemistry—is rarely found today,
particularly within a single facility,” he explains.
That is
precisely what makes the LAUX process unique—it directly intertwines
organic and inorganic chemistry. In a joint reaction, metallic iron is
converted into iron oxide—in conjunction with the reaction of an
organic starting material.
The fact that the facility is still
referred to as a reduction plant has historical reasons. “Actually, we
produce iron oxide pigments—in other words, we oxidize iron,” explains
Friedrich. “The name comes from the fact that, through this oxidation,
we simultaneously reduce nitrobenzene to aniline.” Because in the
beginning, the focus wasn’t on the pigment at all. When the process was
developed in the early 20th century, aniline—which was needed to
produce synthetic dyes—was considered a valuable substance. The iron
oxide accumulated as sludge, and for a long time no one knew what to do
with it. It wasn’t until the mid-1920s that chemist Julius Laux
recognized the potential of this byproduct—thereby laying the foundation
for industrial iron oxide production.
Reduction Plant – Where Iron Is Turned into Pigment
The
most important raw material for a reduction plant comes from the
automotive industry—which, at first glance, has little to do with
pigments. Iron shavings and metal scrap generated during the machining
of castings are used. “So we were already committed to the circular
economy even before the term officially existed,” says Christian
Schütte, who has worked at the company for more than three decades and
is in charge of raw materials procurement. "Sustainability has always
been an integral part of our process."
However, not all waste is
the same: “The quality of the iron we receive clearly plays a key role
in determining the quality of the pigment,” explains the expert. In a
huge warehouse, varieties with different grain sizes and qualities are
therefore mixed together to produce the best possible raw material. The
material is then mechanically processed in the grinding mills, graded,
and prepared for the production process. In the reduction plant, the
actual reaction then proceeds almost entirely automatically. This
reaction is highly exothermic—meaning it releases large amounts of heat.
This energy is put to good use: to generate steam and hot water for the
plant’s own processes, as well as for other plants on the site. “In a
sense, we’re IPG’s boiler room,” says Schütte.
From a Liquid Substance to a Solid Pigment
At
the end of the process, the iron oxide leaves the reduction plant as an
aniline-free paste—thick and completely free of any harmful substances.
It is then transported via pipe bridges to the next facility: pastes
and calcination. “This is where the product takes shape,” says plant
manager Bartholomäus Luczak. “We turn the sludgy mass into a solid
material.”
In terms of area, pastes and calcination is the
largest facility in the Chempark: six large main buildings, five control
rooms, and an extensive network of pipelines covering an area of about 5
hectares. Here, the thick paste is cleaned of iron residues, thickened,
washed, and then dried. Then the next step depends on the color: Black
or yellow pigments are produced directly from the process. To produce
the red pigments, the black paste is then calcined—in other words,
heat-treated.
This process takes place in the massive rotary
kilns located in a separate section of the building, where temperatures
reach up to 900 degrees Celsius. Regina Müller, assistant shift
supervisor, is currently making her rounds there. It’s not just the
scale that’s impressive—the entire atmosphere is striking as well. Over
the years, the massive furnaces, pipes, and equipment have taken on the
red color of the pigment calcined here. “It’s usually much warmer here,”
she explains. “But our kilns are currently being serviced.”
Not Clean, but Colorful
Maintenance
is generally an important issue for the Uerdingen team. The pigment is
highly abrasive—screw conveyors, pipes, and equipment are subjected to
enormous levels of stress during continuous operation. Equipment must
therefore be inspected, serviced, and maintained on a regular basis.
“Despite automation, you spend a lot of time moving around the plant,
switching lines, and sometimes intervening manually,” says Müller.
“That’s what makes the job so interesting to me.”
It goes
without saying that the pigments don’t just color the hall and its
surroundings—by the end of their shift, workers’ clothes bear visible
traces of the product. “You don’t leave our plant clean,” says Müller,
“but you do leave colorful.”
A Strong Whole — for 100 Years
After
passing through the paste and calcination stages, the pigment’s journey
still isn’t over. “We hand it off to our colleagues in the grinding
department,” explains Müller. Here, the pigment undergoes further
processing—it is mixed and either finely ground for its intended
application or compacted into a low-dust form, depending on how and for
what purpose it will later be used by the customer.
The closely
integrated production network is one of the reasons why the process
remains successful even after 100 years—and why it isn’t used anywhere
else in the world. "Many process steps, long distances, large
quantities. Material flows must be coordinated, and turnaround times
must be met—around the clock. “It would be hard to imagine a single
plant being able to handle this,” says Luczak. For Friedrich, too,
close, collaborative partnership is crucial: “No matter which plant—we
always say we make iron oxide together.” This team spirit, combined with
100 years of experience, isn’t something you can just copy.”
Tradition with a Future
100 years of experience—the IPG BU wants to use this to tap into new market potential.
Mr.
Ertl, LANXESS has been producing iron oxide pigments in
Krefeld-Uerdingen using the LAUX process for 100 years. Why is it so
successful?
The inventor of the process, Julius Laux, asked a
surprisingly modern question some 100 years ago: What if waste wasn’t
waste? It all began with the production of aniline from nitrobenzene and
scrap iron—a process that generated large quantities of iron oxide as a
byproduct. Laux realized that, under certain conditions, this iron
oxide is particularly colorful and pure and is suitable as a
high-quality pigment. To this day, the process is considered one of the
most sustainable methods for producing iron oxide pigments. The
combination of recycling metal waste and energy-efficient process steps
has made the LAUX process a key factor in our success.
But you don’t just produce pigments in Germany, do you? How important is the global production network to IPG?
Extremely
important. We have locations on all five continents. Here in Europe, we
still process pigments in Spain and England, as well as in the United
States, Brazil, China, and Australia. This geographic diversification is
a key advantage, as it enables us to improve our delivery capabilities
and makes us more resilient to trade conflicts, sanctions, export
restrictions, political instability, or regional crises. At the same
time, it is important that Germany remains a competitive location for
businesses—especially when it comes to energy costs, which play a key
role in our energy-intensive production. That’s why we’re further
advancing energy optimization through targeted investments in our plants
and processes.
100 years of tradition—where are innovations emerging right now?
We
need a wide range of applications to keep our plants running at full
capacity. That’s why we’re constantly tapping into new markets—even
beyond traditional coloring applications. Battery technology is a
perfect example. In addition to iron oxides, iron phosphates can also be
used in the manufacture of lithium iron phosphate batteries. Following
the successful production of iron phosphate at the pilot plant, IPG is
now developing the large-scale process that will be implemented in the
production facility. This market is growing rapidly worldwide, so we are
actively advancing research in this area. Currently, LFP cathode
materials and the corresponding batteries are primarily produced in
China. So far, there hasn’t been enough capacity in Europe —and we want
to change that.
Highlights
•
Over the past 100 years, the business unit has produced approximately
15 million metric tons of pigment—enough to cover the entire area of
Germany five times over in black, red, and yellow.
• A total of about 100 different shades can be created from the primary colors red, black, yellow, brown, and orange.
• With Bayferrox®, LANXESS is one of the world’s leading suppliers of iron oxide pigments.
• In the construction industry, the Bayferrox® brand is synonymous with iron oxide pigments, much like Kleenex is for tissues.